A simple low-temperature adiabatic calorimeter for small samples

A simple adiabatic calorimeter has been made to investigate the heat capacity of small samples (≤ 1 cm³) of carbon nanomaterials in the temperature range from 1 to 300 K. It makes possible: i) short-time mounting of a sample; ii) doping of samples with gases directly in the calorimeter; iii) short-t...

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Datum:2011
Hauptverfasser: Bagatskii, M.I., Sumarokov, V.V., Dolbin, A.V.
Format: Artikel
Sprache:English
Veröffentlicht: Фізико-технічний інститут низьких температур ім. Б.І. Вєркіна НАН України 2011
Schriftenreihe:Физика низких температур
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Online Zugang:http://dspace.nbuv.gov.ua/handle/123456789/118551
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Назва журналу:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Zitieren:A simple low-temperature adiabatic calorimeter for small samples / M.I. Bagatskii, V.V. Sumarokov, A.V. Dolbin // Физика низких температур. — 2011. — Т. 37, № 5. — С. 535–538. — Бібліогр.: 4 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
Beschreibung
Zusammenfassung:A simple adiabatic calorimeter has been made to investigate the heat capacity of small samples (≤ 1 cm³) of carbon nanomaterials in the temperature range from 1 to 300 K. It makes possible: i) short-time mounting of a sample; ii) doping of samples with gases directly in the calorimeter; iii) short-time cooling of a sample down to helium temperatures. The adiabatic calorimeter is suitable to place into a helium vessel of a portable Dewar or a helium cryostat. The heat capacity of the fullerit sample has been measured in the temperature range from 1 to 30 K.