Investigation of metal β-diketonates as parent materials for reference samples

Stability of synthesized lead, cadmium and chromium (III) β-diketonates and mercury (I) dimedonate in solid state and in diluted solutions was investigated by titrimetry and inductively coupled plasma optical emission spectrometry. It was shown, that the solid samples are stable during 5 years and...

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Datum:2005
Hauptverfasser: Yurchenko, O.I., Shevtsov, N.I., Mikhailova, L.I., Belikov, K.N., Titova, N.P., Shkumat, A.A.
Format: Artikel
Sprache:English
Veröffentlicht: НТК «Інститут монокристалів» НАН України 2005
Schriftenreihe:Functional Materials
Online Zugang:http://dspace.nbuv.gov.ua/handle/123456789/138855
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Назва журналу:Digital Library of Periodicals of National Academy of Sciences of Ukraine
Zitieren:Investigation of metal β-diketonates as parent materials for reference samples / O.I. Yurchenko, N.I. Shevtsov, L.I. Mikhailova, K.N. Belikov, N.P. Titova, A.A. Shkumat // Functional Materials. — 2005. — Т. 12, № 2. — С. 405-408. — Бібліогр.: 22 назв. — англ.

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Digital Library of Periodicals of National Academy of Sciences of Ukraine
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spelling irk-123456789-1388552018-06-20T03:05:53Z Investigation of metal β-diketonates as parent materials for reference samples Yurchenko, O.I. Shevtsov, N.I. Mikhailova, L.I. Belikov, K.N. Titova, N.P. Shkumat, A.A. Stability of synthesized lead, cadmium and chromium (III) β-diketonates and mercury (I) dimedonate in solid state and in diluted solutions was investigated by titrimetry and inductively coupled plasma optical emission spectrometry. It was shown, that the solid samples are stable during 5 years and the solutions keep the concentration for 4 months. Metal acetylacetonates are recommended as parent substances for manufacturing of reference samples used for calibration of analytical instruments and accuracy control. Исследована устойчивость синтезированных β-дикетонатов свинца, кадмия, хрома (III) и димедоната ртути (I) в твердом состоянии и в разбавленных растворах методами титриметрического анализа и атомно-эмиссионной спектрометрии с индукционной плазмой. Показано, что твердые образцы устойчивы в течение 5 лет, а разбавленные растворы сохраняют свою концентрацию 4 месяца. Ацетилацетонаты металлов рекомендованы в качестве исходных веществ для изготовления стандартных образцов состава при градуировке аналитических приборов и контроля правильности результатов анализа. Дослiджено стiйкiсть синтезованих β-дикетонатiв свинцю, кадмiю, хрому (III) та димедонату ртутi (I) у твердому станi та у розведених розчинах методами титриметричного аналiзу та атомно-емiсiйної спектрометрiї з iндукцiйною плазмою. Показано, що твердi зразки є стiйкими на протязi 5 рокiв, а розведенi розчини зберiгають концентрацiю 4 мiсяцi. Ацетилацетонати металiв рекомендовано як вихiднi речовини для виготовлення стандартних зразкiв складу при градуюваннi аналiтичних приладiв та проведеннi контролю правильностi результатiв аналiзу. 2005 Article Investigation of metal β-diketonates as parent materials for reference samples / O.I. Yurchenko, N.I. Shevtsov, L.I. Mikhailova, K.N. Belikov, N.P. Titova, A.A. Shkumat // Functional Materials. — 2005. — Т. 12, № 2. — С. 405-408. — Бібліогр.: 22 назв. — англ. 1027-5495 http://dspace.nbuv.gov.ua/handle/123456789/138855 en Functional Materials НТК «Інститут монокристалів» НАН України
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
language English
description Stability of synthesized lead, cadmium and chromium (III) β-diketonates and mercury (I) dimedonate in solid state and in diluted solutions was investigated by titrimetry and inductively coupled plasma optical emission spectrometry. It was shown, that the solid samples are stable during 5 years and the solutions keep the concentration for 4 months. Metal acetylacetonates are recommended as parent substances for manufacturing of reference samples used for calibration of analytical instruments and accuracy control.
format Article
author Yurchenko, O.I.
Shevtsov, N.I.
Mikhailova, L.I.
Belikov, K.N.
Titova, N.P.
Shkumat, A.A.
spellingShingle Yurchenko, O.I.
Shevtsov, N.I.
Mikhailova, L.I.
Belikov, K.N.
Titova, N.P.
Shkumat, A.A.
Investigation of metal β-diketonates as parent materials for reference samples
Functional Materials
author_facet Yurchenko, O.I.
Shevtsov, N.I.
Mikhailova, L.I.
Belikov, K.N.
Titova, N.P.
Shkumat, A.A.
author_sort Yurchenko, O.I.
title Investigation of metal β-diketonates as parent materials for reference samples
title_short Investigation of metal β-diketonates as parent materials for reference samples
title_full Investigation of metal β-diketonates as parent materials for reference samples
title_fullStr Investigation of metal β-diketonates as parent materials for reference samples
title_full_unstemmed Investigation of metal β-diketonates as parent materials for reference samples
title_sort investigation of metal β-diketonates as parent materials for reference samples
publisher НТК «Інститут монокристалів» НАН України
publishDate 2005
url http://dspace.nbuv.gov.ua/handle/123456789/138855
citation_txt Investigation of metal β-diketonates as parent materials for reference samples / O.I. Yurchenko, N.I. Shevtsov, L.I. Mikhailova, K.N. Belikov, N.P. Titova, A.A. Shkumat // Functional Materials. — 2005. — Т. 12, № 2. — С. 405-408. — Бібліогр.: 22 назв. — англ.
series Functional Materials
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AT shevtsovni investigationofmetalbdiketonatesasparentmaterialsforreferencesamples
AT mikhailovali investigationofmetalbdiketonatesasparentmaterialsforreferencesamples
AT belikovkn investigationofmetalbdiketonatesasparentmaterialsforreferencesamples
AT titovanp investigationofmetalbdiketonatesasparentmaterialsforreferencesamples
AT shkumataa investigationofmetalbdiketonatesasparentmaterialsforreferencesamples
first_indexed 2025-07-10T06:43:43Z
last_indexed 2025-07-10T06:43:43Z
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