Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan

Various magnetic properties of magnetic minerals show strong grain-size depen-dence. This dependency occurs because these parameters are influenced by the magnetic grain-size (domain state) of the samples. Natural rocks often contain a mixture of different magnetic minerals with different grain-size...

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Автор: Novruzov, Z.A.
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Опубліковано: Інститут геофізики ім. С.I. Субботіна НАН України 2019
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Цитувати:Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan / Z.A. Novruzov // Геофизический журнал. — 2019. — Т. 41, № 3. — С. 203-210. — Бібліогр.: 5 назв. — англ.

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spelling irk-123456789-1585472019-09-05T01:26:20Z Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan Novruzov, Z.A. Various magnetic properties of magnetic minerals show strong grain-size depen-dence. This dependency occurs because these parameters are influenced by the magnetic grain-size (domain state) of the samples. Natural rocks often contain a mixture of different magnetic minerals with different grain-size (domain states). Thus determination of the domain state is important. The Saatly ultradeep well’s volcanics were used as a research material. In the depth intervals of 3540—8126 m the volcanics had been revealed by the borehole. Магнитные свойства различных магнитных минералов очень зависят от размера зерен (доменного состояния). Горные породы часто содержат смесь различных магнитных минералов с различными размерами зерен (доменных состояний). В качестве материала для определения доменного состояния зерен минералов использовано вулканиты с сверхглубокой скважины Саатлы в интервале глубин 3540-8126 м. Магнітні властивості різних магнітних мінералів дуже залежать від розміру зерен (доменного стану). Гірські породи часто містять суміш різних магнітних мінералів з різними розмірами зерен (доменних станів). Як матеріал для визначення доменного стану зерен мінералів використано вулканіти з надглибокої свердловини Саатлі в інтервалі глибин 3540—8126 м. 2019 Article Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan / Z.A. Novruzov // Геофизический журнал. — 2019. — Т. 41, № 3. — С. 203-210. — Бібліогр.: 5 назв. — англ. 0203-3100 DOI: 10.24028/gzh.0203-3100.v41i3.2019.172474 http://dspace.nbuv.gov.ua/handle/123456789/158547 538.245+550.382):551.24:552(622.241:479.24 en Геофизический журнал Інститут геофізики ім. С.I. Субботіна НАН України
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
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description Various magnetic properties of magnetic minerals show strong grain-size depen-dence. This dependency occurs because these parameters are influenced by the magnetic grain-size (domain state) of the samples. Natural rocks often contain a mixture of different magnetic minerals with different grain-size (domain states). Thus determination of the domain state is important. The Saatly ultradeep well’s volcanics were used as a research material. In the depth intervals of 3540—8126 m the volcanics had been revealed by the borehole.
format Article
author Novruzov, Z.A.
spellingShingle Novruzov, Z.A.
Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan
Геофизический журнал
author_facet Novruzov, Z.A.
author_sort Novruzov, Z.A.
title Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan
title_short Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan
title_full Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan
title_fullStr Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan
title_full_unstemmed Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan
title_sort domain structure of volcanics’ ferromagnetic grains: a case study of the saatly ultradeep well, azerbaijan
publisher Інститут геофізики ім. С.I. Субботіна НАН України
publishDate 2019
url http://dspace.nbuv.gov.ua/handle/123456789/158547
citation_txt Domain structure of volcanics’ ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan / Z.A. Novruzov // Геофизический журнал. — 2019. — Т. 41, № 3. — С. 203-210. — Бібліогр.: 5 назв. — англ.
series Геофизический журнал
work_keys_str_mv AT novruzovza domainstructureofvolcanicsferromagneticgrainsacasestudyofthesaatlyultradeepwellazerbaijan
first_indexed 2025-07-14T11:07:31Z
last_indexed 2025-07-14T11:07:31Z
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fulltext DOMAIN STRUCTURE OF VOLCANICS� FERROMAGNETIC GRAINS ... AZERBAIJAN Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 203 Domain structure of volcanics� ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan Z. A. Novruzov, 2019 Institute of Geology and Geophysics of NAS of Azerbaijan, Baku, Azerbaijan Received 21 November 2018 Ìàãí³òí³ âëàñòèâîñò³ ð³çíèõ ìàãí³òíèõ ì³íåðàë³â äóæå çàëåæàòü â³ä ðîçì³ðó çå- ðåí (äîìåííîãî ñòàíó). óðñüê³ ïîðîäè ÷àñòî ì³ñòÿòü ñóì³ø ð³çíèõ ìàãí³òíèõ ì³íå- ðàë³â ç ð³çíèìè ðîçì³ðàìè çåðåí (äîìåííèõ ñòàí³â). ßê ìàòåð³àë äëÿ âèçíà÷åííÿ äî- ìåííîãî ñòàíó çåðåí ì³íåðàë³â âèêîðèñòàíî âóëêàí³òè ç íàäãëèáîêî¿ ñâåðäëîâèíè Ñààòë³ â ³íòåðâàë³ ãëèáèí 3540�8126 ì. Çà äàíèìè ïåòðîãðàô³÷íîãî òà åëåêòðîííî- ì³êðîñêîï³÷íîãî àíàë³ç³â ó âåðõí³é ÷àñòèí³ ðîçð³çó (3540�5500 ì) öèõ ïîð³ä çåðíà ðóäíèõ ì³íåðàë³â ïðåäñòàâëåí³ äâîìà ãåíåðàö³ÿìè: 1) âåëèê³ çåðíà òèòàíîìàãíåòè- òó (á³äí³ íà òèòàí), ãîìîãåíí³ àáî ç³ ñòðóêòóðàìè ðîçïàäó; 2) íåâåëèê³ çà ðîçì³ðîì, çàçâè÷àé äîáðå îãðàíîâàí³ çåðíà ïðàêòè÷íî ñòåõ³îìåòðè÷íîãî ìàãíåòèòó. Ãîìîãåíí³ íåâåëèê³ çåðíà àáî ôðàãìåíòè ðîçïàäó âåëèêèõ çåðåí (ÿê³ äóæå çì³íåí³ õ³ì³÷íî) ìî- æóòü ìàòè âëàñòèâîñò³ îäíîäîìåííèõ ÷àñòèíîê; ôåðîìàãí³òí³ çåðíà ÷àñòî âèçíà÷à- þòü ÿê ïñåâäîîäèíè÷íèé äîìåí. Ó íèæí³é ÷àñòèí³ ðîçð³çó (5500�8126 ì) ìóëüòèäî- ìåíí³ çåðíà òèòàíîìàãíåòèòó çá³äíåí³ òèòàíîì. Ç ãëèáèí 7000 ì ñïîñòåð³ãàºòüñÿ òà- êîæ îêèñíåíèé ìàãíåòèò. Ïñåâäîîäíîäîìåííèõ çåðåí çàô³êñîâàíî çíà÷íî ìåíøå, í³æ ó âåðõí³é ÷àñòèí³ ðîçð³çó. Ç ãëèáèíè 7300 ì ³ íèæ÷å âîíè ïîâí³ñòþ â³äñóòí³. Çà ðåçóëüòàòàìè äîñë³äæåíü, ôåðîìàãíåòèê ïðåäñòàâëåíèé ³ñòîòíî ìóëüòèäîìåííèìè çåðíàìè. Ñë³ä çàçíà÷èòè, ùî êðèòåð³é Ëîð³�Ôóëëåðà íåïðèäàòíèé ïðè ³äåíòèô³- êàö³¿ äîìåííî¿ ñòðóêòóðè ñêëàäíîãî ñïîëó÷åííÿ ôåðîìàãí³òíèõ çåðåí. Êëþ÷îâ³ ñëîâà: íåïðÿì³ ìàãí³òí³ êðèòåð³¿, ìàãí³òíèé äîìåííèé ñòàí, âóëêàíîãåí- í³ ïîðîäè, íàäãëèáîêà ñâåðäëîâèíà. Introduction. For the first time magne- tometric researches of volcanogenic rock co- re of the super deep Saatly well have been conducted by the staff of department �Geo- magnetism� of the Institute of Geology and Geophysics of Azerbaijan National Acade- my of Science (ANAS). The necessity in the magnetic researches of a core of the Saat- ly super deep well has been dictated by ne- ed in obtaining the petromagnetic data used at interpretations of results of geophysical activity. The ore minerals� magnetic research together with microprobe analysis of them [Novruzov, Tselmovich, 2018] revealed that magnetic properties of rocks are bound with magnetite and Ti-poor titanomagnetite. Environmental conditions of generation of ferromagnetic minerals and changes of them leave traces on magnetic domain struc- ture [Stackey, Banerjee, 1974]. Application of the rock magnetic method for identifica- tion of domain structure of magnetic grains is the purpose of the proposed article. For realization of this purpose we used four mag- netic criteria. The criteria are based on cha- racteristics of various magnetic parameters of magnetic grains with different magnetic domain structures. Description of the object. The superde- ep well is located near the city of Saatly (λ = = 39.91 °N, ϕ = 48.36 °E), Azerbaijan (Fig. 1). The region of the well location (design depth DOI: https://doi.org/10.24028/gzh.0203-3100.v41i3.2019.172474 ÓÄÊ (538.245+550.382):551.24:552(622.241:479.24) Z. A. NOVRUZOV 204 Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 of 15 km) is spaced in the Kur basin placed between the Greater Caucasus and the Les- ser Caucasus (the large tectonic construc- tions). According to deep structure the Kur basin is subdivided into three depressions: upper Kura basin, middle Kura basin and lower Kura basin. The Saatly superdeep well is located within the middle Kura basin. According to geophysical data interpre- tation the crystalline basement (around the Saatly local gravitational maximum) posses- ses a block structure (where there are rocks of persilicic and basic composition at a depth of 8 km). Debatable idea of crustal structu- re within the Saatly local gravitational maxi- mum was formed in two points of view. Ac- cording to the first � the Earth crust con- sists of granite and basalt layers, according to the second � the Earth crust is single- layer and it is presented by mafic rocks on- ly. Features of the Earth crust and the redu- ced thickness of a sedimentary cover at Sa- atly territory formed a basis for drilling of the super deep well. Object of our researches are the volca- nics located in the depths interval of 3540� 8126 m. According to research papers [Ab- dullaev, Salakhov, 1983; Abdullaev et al. , 1984] the development of the low-tempera- ture metamorphism (depth of 3540�7000m) has been noted in the volcanogenic rocks. But from depths of 7000 m and deeper the development of the low-temperature meta- somatism is revealed. The quantities of the studied volcanic rocks were 49. Three dup- licate with cubic form (1 cm) were sawn from each sample. The depth interval of 3540�3900m is cha- racterized by plagioclase basalts and is ma- inly presented by volcanogenic facies. Ba- salts contain the potassium-enriched and so- dium-enriched alkalinity. The depth interval of 3900�4850 m con- tains porphyritic olivine-pyroxene-plagio- clase-basalts and pyroxene-plagioclase-ba- salts. Basalts are low-alkaline (low-potassium). The depth interval of 4850�5209 m pos- sesses much bigger phases of rocks. Except Fig. 1. The Saatly super deep well location. DOMAIN STRUCTURE OF VOLCANICS� FERROMAGNETIC GRAINS ... AZERBAIJAN Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 205 basalts their amfibole-contaning phases and andesites are noted. Along with low-potas- sium basalts potassium-enriched groups ha- ve been discovered. In the depth interval of 5209�6100m the double-pyroxene-plagioclase basalts and an- desite-basalts prevail. These rocks possess the alkalescence and the strong fracturing. There are andesites in the depth interval of 6100�6800 m. The microdolerite sills are noted as well. Upper parts of 6800�8000m depth inter- val are presented by dacites, dacite-tuffs and pumiceous breccia. In the middle horizons and lower ones of the interval dacites are al- ternating with plagiorhyolite and andesites. Thus, the studied columnvolcanics chan- ge with depth: from the mafics (andesite-ba- salts, basalts) to intermediate rocks (andesi- tes) and then to persilicrocks (rhyodacites, dacites). Technique of works. During the magne- tic researches of volcanogenic rocks of the superdeep Saatly well the following magne- tic parameters were measured: a natural re- manent magnetization (NRM ) and magne- tic susceptibility (χ ). At the laboratory on each duplicate sample (for each one the NRM and the χ were measured) saturation isother- mal remanent magnetization (SIRM) and iso- thermal remanent magnetization (IRM) in the field of 1.5 T have been created. At the la- boratory a thermal remanent magnetizati- on (TRM) was created on each duplicate of sample by means of cooling from tempera- tures above the Curie point (more than 600 °C) in the presence of magnetic field equal to 0.5 ⋅ 10–4 Ò. Partial thermal remanent mag- netizations (PTRM) were created from tem- peratures 200�500 °C (mainly from 200 °C) to 20 °C in the field of 0.5 ⋅ 10–4 Ò. Saturation isothermal remanent magneti- zation (SIRM), isothermal remanent magne- tization (IRS) and the thermoremanent mag- netization (TRM) were measured at the labo- ratory. All laboratory measurements were car- ried out at the laboratory of �The main geo- magnetic field and a petromagnetizm� of the Institute of Physics of Solid Earth of RAS. Natural remanent magnetization (NRM) and thermal remanent magnetization (TRM) we- re measured on a magnetometer JR-4 (Brno, Czech Republic). SIRM (Mrs) was measured on an automatic thermomagnetometer with sensitivity 1 ⋅ 10–4 A/m. A saturation magne- tization (Ms) was measured on a vibromag- netometer with sensitivity 1 ⋅ 10–1 A/m. The magnetic susceptibility was measured on a Kappabridge KLY -2 (Brno, Czech Republic). Stepwise demagnetization by increasing alternating field was carried out on the RUV semi-automatic installation in the range of fields of 0�80 A/m. The PTRM were ther- mally demagnetized by a routine technique [Kobayashi, Fuller, 1967]. Results of the researches. Magnetic re- searches of the well volcanogenic rocks sho- wed that the measured magnetic parame- ters of Mrs and Ms and TRM and Qn are changing according to depth. Changes of these parameters reflect variations of grain size. Magnetic parameters of NRM, χ, SIRM (Mrs), Ms and TRM were measured for study of a minerals� magnetic domain state of the Saatly superdeep well. There are three types of different magnetic behavior, depending on the grain size. The defined parameters allowed calculating Qn factor and magni- tude of Mrs /Ms. For use of magnetothermal criterion the partial thermal remanent magnetizations (PTRM) were created. The PTRM were acquired in the range of temperatures 200�500 °C. For identification of a magnetic domain state of volcanic ferromagnetic grains of the Saatly well the four magnetic criteria were used: factor Qn, Mrs /Ms, Lauri-Fuller�s criterion and thermal magnetic criterion. Short consideration of identification cri- teria of a magnetic domain state had bro- ught to light that that any of criteria does not work completely well , even in case of ensembles of �pure� grains. The found struc- tural heterogeneities of grains [Novruzov, Tselmovich, 2018] and also grains various by structure and the sizes (magnetic rese- arches of the structure and concentration) make impossible to use only one of the men- tioned criteria. Therefore in this article, the Z. A. NOVRUZOV 206 Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 The experimental results of definition of a magnetic domain structure of ferromagnetic grains of volcanogenic rocks of the Saatly well section (interval of 3540�8126 m) Criterion Type of rock Depts, m Qn Domain state M rs /M s Domain state Lauri� Fuller Thermo- mag- netic Total Andesite- basalt 3540�3546 0,15 MD 0,04 SD � MD MD Basalt 3660�3666 2,03 PSD 0,26 SD (PSD) � MD MD (PSD) Basalt 3761�3767 0,29 MD 0,17 PSD SD MD MD Basalt 3820�3825 0,51 MD 0,13 PSD SD � MD (PSD) Basalt 3975�3981 1,71 PSD 0,13 PSD SD � PSD Basalt 4062�4067 0,33 MD 0,10 PSD ? � MD (PSD) Basalt 4165�4171 2,55 PSD 0,24 PSD SD MD PSD Basalt 4250�4255 0,41 MD 0,12 PSD SD MD MD (PSD) Basalt 4310�4315 0,18 MD 0,04 MD SD MD MD Andesite- basalt 4423�4428 0,31 MD 0,07 MD (PSD) SD � MD Basalt 4516�4522 0,83 MD 0,06 MD (PSD) SD � MD Basalt 4600�4608 1,30 PSD 0,03 MD SD MD MD (PSD) Basalt 4634�4640 0,68 MD 0,07 MD (PSD) SD MD MD Basalt 4686�4692 0,74 MD 0,08 MD (PSD) SD MD MD Dolerite 4714�4719 0,32 MD 0,07 MD (PSD) SD � MD Dolerite 4770�4777 0,81 MD 0,05 MD SD MD MD Andesite- basalt 4800�4807 1,82 PSD 0,04 MD MD � MD Andesite- basalt 4881�4885 0,60 MD 0,02 MD SD � MD Basalt 4915�4922 1,39 PSD 0,02 MD SD MD MD (PSD) Andesine 5036�5040 0,30 MD 0,04 MD SD MD MD Gabbros- norite 5129�5132 0,35 MD 0,06 MD (PSD) SD MD MD Basalt 5185�5190 0,69 MD 0,03 MD SD MD MD Basalt 5270�5273 3,00 PSD 0,06 MD (PSD) SD MD MD (PSD) Basalt 5385�5390 1,40 PSD 0,04 MD SD � MD (PSD) most often used in rock magnetism the four criteria are applied. At the same time the judgment of a magnetic domain state was based on coincidence of results of identifi- cation by the two or the three criteria. The results of identification of a magne- tic domain state of the ferromagnetic grains are presented in Table. In Fig. 2 and Fig. 3 typical demagnetization curves of TRM and SIRM in alternating magnetic field (Lauri- DOMAIN STRUCTURE OF VOLCANICS� FERROMAGNETIC GRAINS ... AZERBAIJAN Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 207 SD � single-domain particles; PSD � pseudo-single-domain particles; MD � multi-domain particles. Continuation of Table Basalt 5467�5474 0,53 MD 0,05 MD SD � MD Andesite 5544�5550 1,89 PSD 0,07 MD (PSD) SD MD MD (PSD) Basalt 5634�5636 5,95 PSD 0,08 MD (PSD) SD MD MD (PSD) Andesite- basalt 5746�5750 2,12 PSD 0,11 PSD SD MD PSD Andesite 5828�5830 5,48 PSD 0,08 MD (PSD) SD MD MD (PSD) Andesite 6000�6003 1,36 PSD 0,07 MD (PSD) SD � MD (PSD) Andesite 6174�6178 0,68 MD 0,03 MD ? � MD Andesite- basalt 6290�6295 1,00 MD 0,05 MD ? � MD Andesite 6430�6435 1,00 MD (PSD) 0,07 MD (PSD) SD � MD (PSD) Andesite 6581�6583 1,72 PSD 0,08 MD (PSD) SD MD0 MD (PSD) Andesite- basalt 6740�6745 2,90 PSD 0,03 MD SD � MD (PSD) Andesite 6877�6882 1,15 MD (PSD) 0,06 MD (PSD) SD � MD (PSD) Dolerite 6994�7003 1,87 PSD 0,13 PSD SD MD MD (PSD) Dacite 7038�7048 0,50 MD 0,07 MD (PSD) MD � MD Dacite 7172�7176 2,15 PSD 0,05 MD (PSD) SD � MD (PSD) Rhyodacite 7264�7276 0,29 MD 0,31 SD (PSD) SD � MD (PSD) Dolerite 7332�7343 0,49 MD 0,03 MD SD � MD Rhyodacite 7420�7428 0,50 MD 0,04 MD SD MD MD Dacite 7576�7578 0,85 MD 0,06 MD (PSD) SD MD MD Dacite 7642�7646 0,25 MD 0,04 MD ? � MD Dacite 7729�7738 1,77 PSD 0,05 MD (PSD) SD MD MD Rhyodacite 7874�7878 0,21 MD 0,02 MD SD MD MD Andesite- dacite 7991�7993 0,65 MD 0,04 MD SD MD MD Rhyolite 8103�8108 0,57 MD 0,03 MD SD MD MD Dacite 8108�8126 0,80 MD 0,05 MD SD � MD Fuller�s criterion) are represented. In Fig. 4 typical thermal demagnetization curves of PTRM acquired at different temperatures (ther- mal magnetic criterion) are presented. We can see in the table that in most ca- ses grains of magnetic minerals (carriers of remanent magnetization), are in a multido- main state. For an upper part of a section of volcanogenic rocks (3540�5500 m), espe- cially in the depth interval of 3540�5000m, Z. A. NOVRUZOV 208 Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 the pseudo-single-domain state often beco- mes apparent. It demonstrates that rema- nent magnetization carriers in this interval of depths are the finest grains. These grains, most probably, belong, to the second gene- ration of grains of magnetite and the Ti-po- or titanomagnetite determined on the basis of microprobe analysis [Novruzov, Tselmo- vich, 2018]. In the bottom of a section (5500�8126m) is more often, and in the depth interval 7300� 8126 m one and all studied rocks contain only multidomain grains of ferromagnetic minerals. This result presumably can be bound to that circumstance that the low-temperature metamorphism, especially metasomatism, results in partial or complete collapse (repla- cement) of fine grains of the ferromagnetic minerals in the bottom of a section which are contained in rocks. At the same time artificial �enrichment� of rocks with more coarse magnetic grains is observed. As shown by means of micro- probe [Novruzov, Tselmovich, 2018] of ore grains the fine fraction of the deepest rocks is presented, mainly, by fragments of the crushed large grains. Discussion of results. The done petro- magnetic researches showed that in most cases grains of magnetic minerals (carriers of remanent magnetization) represent an en- semble of multidomain particles. In upper part of the section (3540�5500), especially in the depth interval 3540�5000 m, the pse- udo-single domain state is often presented. It demonstrates that in this depth interval, except of course (large volume) multidoma- in grain generation, fine grains of other gene- ration can bear a remanent magnetization. The results of identification of a domain structure presented in the summary table, in the deeper section (5500�8126 m) are more often, and in the depth interval 7300� 8126 m one and all ferromagnetic minerals are demonstrating only multidomain grains content. This result presumably can be ca- used by the fact that in the deeper section the generation (rather) of fine ferromagne- tic grains can be partially or entirely destro- yed due to occurrence of the low-tempera- ture metamorphism (metasomatism). As a re- Fig. 2. The alternating magnetic field demagne- tization curves (TRM and SIRM) as Lauri-Fuller�s criterion for upper part of section. Fig. 4. Thermal demagnetization of the PTRM as thermomagnetic criterion of identification of type of domain state. Fig. 3. The alternating magnetic field demagne- tization curves (TRM and SIRM) as Lauri-Fuller�s criterion for bottom part of section. DOMAIN STRUCTURE OF VOLCANICS� FERROMAGNETIC GRAINS ... AZERBAIJAN Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 209 sult the share of the ferrimagnetic coarse grains possessing a multidomain structure increases. As is obvious from the table the Lauri- Fuller�s criterion is inapplicable for the com- plex ensemble of ferromagnetic grains. Use of this criterion eventuates in the diametri- cally opposite data received on the basis of the two or the three other criteria of doma- in structure identificationThe thermal mag- netic criterion is sensitive to manifestation of single-domain (pseudo-single-domain) and of multidomain ferromagnetic grains of in the complex ensemble of grains. Domain structure of volcanics� ferromagnetic grains: A case study of the Saatly ultradeep well, Azerbaijan Z. A. Novruzov, 2019 Various magnetic properties of magnetic minerals show strong grain-size depen- dence. This dependency occurs because these parameters are influenced by the magne- tic grain-size (domain state) of the samples. Natural rocks often contain a mixture of dif- ferent magnetic minerals with different grain-size (domain states). Thus determination of the domain state is important. The Saatly ultradeep well�s volcanics were used as a re- search material. In the depth intervals of 3540�8126 m the volcanics had been revea- led by the borehole. According to data of the petrographic and microprobe analysis the volcanogenics of the ultradeep borehole is conditionally divided into a two parts: 1) the upper part (an interval of depths of 3540�5500 m); 2) the bottom part (an interval of depths of 5500�8126 m). In the upper part of section according to microprobe analysis of volcanogenic rocks ore grains are presented by two generations: 1) large grain of ti- tanomagnetites (Ti-poor), homogeneous or with a decay structures; 2) small-sized usual- ly well faced grain of practically stoichiometric magnetite. So, homogeneous small-si- zed grains or fragments of decay large grains (which are strongly changed chemically) can have properties of single-domain particles. Here the ferromagnetic grains (especi- ally in the depth interval 3540�5000 m) are often noted as a pseudo-single domain. In the bottom part of the section the presence of multidomain grains of the Ti-poor titano- magnetite is noted. And since depths of 7000 m the oxidized magnetite is also observed. The pseudo-single-domain grains are fixed much less than in the upper section. And, since a depth mark of 7300 m and deeper, they are absent wholly. In the result of rese- arch it turned out that the ferromagnetic is presented by basically multidomain grains. It should be noted that Lauri-Fuller�s Criterion is not applicable at identification of a domain structure of the complex ensemble of the ferromagnetic grains. Key words: indirect magnetic criteria, magnetic domain state, volcanogenic rocks, super deep well. References Abdullaev, R. N., & Salakhov, A. S. (1983). Com- parative characteristics of Jurassic volcanics Kurdamir-Saatli buried uplift and the north- eastern part of the Lesser Caucasus. Izvestiya AN AzSSR, ser. Nauka o Zemle, (4), 14�23 (in Russian). Abdullaev, R. N., Salayeva, F. O., & Salakhov, A. S. (1984). Magmatic complexes of the Middle Ku- rin depression. In Questions of mineralogy and lithology (pp. 85�90). Baku (in Russian). Kobayashi, K., & Fuller, M. D. (1967). Vibrati- on magnetometer. In D. W. Collinson, K. M. Cre- er, & S. K. Runcorn (Eds.), Methods in palaeo- Z. A. NOVRUZOV 210 Ãåîôèçè÷åñêèé æóðíàë ¹ 3, Ò. 41, 2019 magnetism (pp. 450�456). Amsterdam-Lon- don-New York: Elsevier. Novruzov, Z. A., & Tselmovich, V. A. (2018). Mic- roroentgen spectral ore mineral analysis of Sa- atly column well volcanic (depth interval 3540� 8126 m). Stratigraphy and sedimentology of oil-gas basins (International scientific journal), (2), 70�84. Stackey, F. D., & Banerjee, S. K. (1974). The phy- sical principles of rock magnetism. Amster- dam: Elsevier, 195 p.