Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV

The radiation resistance of Sm-Co and Nd-Fe-B magnets under 10 MeV electron beam was studied. The simulation and design of a magnetic system for electron beam analysis of a technological accelerator for energy up to 10 MeV was carried out. The key component of magnetic system was Sm₂Co₁₇ magnets wit...

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Datum:2019
Hauptverfasser: Bovda, V.A., Bovda, A.M., Guk, I.S., Kandybey, S.S., Kononenko, S.G., Lyashchenko, V.N., Mytsykov, A.O., Onischenko, L.V.
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Zitieren:Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV / V.A. Bovda, A.M. Bovda, I.S. Guk, S.S. Kandybey, S.G. Kononenko, V.N. Lyashchenko, A.O. Mytsykov, L.V. Onischenko // Problems of atomic science and technology. — 2019. — № 2. — С. 145-150. — Бібліогр.: 27 назв. — англ.

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spelling irk-123456789-1949432023-12-01T20:32:33Z Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV Bovda, V.A. Bovda, A.M. Guk, I.S. Kandybey, S.S. Kononenko, S.G. Lyashchenko, V.N. Mytsykov, A.O. Onischenko, L.V. Physics of radiotechnology and ion-plasma technologies The radiation resistance of Sm-Co and Nd-Fe-B magnets under 10 MeV electron beam was studied. The simulation and design of a magnetic system for electron beam analysis of a technological accelerator for energy up to 10 MeV was carried out. The key component of magnetic system was Sm₂Co₁₇ magnets with the size of 30х24х12 mm. The maximum magnetic field in the magnetic system was 0.3 T. Експериментально досліджена радіаційна стійкість магнітних матеріалів зi Sm-Co- і Nd-Fe-B-сплавів під дією 10 МэВ електронного пучка. На основі зразків зi Sm₂Co₁₇-сплаву розмірами 30х24х12 мм проведені моделювання і конструювання магніту для аналізу пучка електронів технологічного прискорювача на енергію 10 МеВ. Приведено результати експериментального дослідження характеристик магніту. Максимальне поле в магніті дорівнює 0,3 Тл. Экспериментально исследована радиационная стойкость магнитных материалов из Sm-Co- и Nd-Fe-B-сплавов под действием 10 МэВ электронного пучка. На основе образцов из Sm₂Co₁₇-сплава размерами 30х24х12 мм проведено моделирование и конструирование магнита для анализа пучка электронов технологического ускорителя на энергию 10 МэВ. Приведены результаты экспериментального исследования характеристик магнита. Максимальное поле в магните равно 0,3 Тл. 2019 Article Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV / V.A. Bovda, A.M. Bovda, I.S. Guk, S.S. Kandybey, S.G. Kononenko, V.N. Lyashchenko, A.O. Mytsykov, L.V. Onischenko // Problems of atomic science and technology. — 2019. — № 2. — С. 145-150. — Бібліогр.: 27 назв. — англ. 1562-6016 PACS: 29.30.Kv http://dspace.nbuv.gov.ua/handle/123456789/194943 en Вопросы атомной науки и техники Національний науковий центр «Харківський фізико-технічний інститут» НАН України
institution Digital Library of Periodicals of National Academy of Sciences of Ukraine
collection DSpace DC
language English
topic Physics of radiotechnology and ion-plasma technologies
Physics of radiotechnology and ion-plasma technologies
spellingShingle Physics of radiotechnology and ion-plasma technologies
Physics of radiotechnology and ion-plasma technologies
Bovda, V.A.
Bovda, A.M.
Guk, I.S.
Kandybey, S.S.
Kononenko, S.G.
Lyashchenko, V.N.
Mytsykov, A.O.
Onischenko, L.V.
Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV
Вопросы атомной науки и техники
description The radiation resistance of Sm-Co and Nd-Fe-B magnets under 10 MeV electron beam was studied. The simulation and design of a magnetic system for electron beam analysis of a technological accelerator for energy up to 10 MeV was carried out. The key component of magnetic system was Sm₂Co₁₇ magnets with the size of 30х24х12 mm. The maximum magnetic field in the magnetic system was 0.3 T.
format Article
author Bovda, V.A.
Bovda, A.M.
Guk, I.S.
Kandybey, S.S.
Kononenko, S.G.
Lyashchenko, V.N.
Mytsykov, A.O.
Onischenko, L.V.
author_facet Bovda, V.A.
Bovda, A.M.
Guk, I.S.
Kandybey, S.S.
Kononenko, S.G.
Lyashchenko, V.N.
Mytsykov, A.O.
Onischenko, L.V.
author_sort Bovda, V.A.
title Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV
title_short Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV
title_full Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV
title_fullStr Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV
title_full_unstemmed Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV
title_sort rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 mеv
publisher Національний науковий центр «Харківський фізико-технічний інститут» НАН України
publishDate 2019
topic_facet Physics of radiotechnology and ion-plasma technologies
url http://dspace.nbuv.gov.ua/handle/123456789/194943
citation_txt Rare-earth permanent magnet in magnetic system of electron accelerator with the energy of 10 MеV / V.A. Bovda, A.M. Bovda, I.S. Guk, S.S. Kandybey, S.G. Kononenko, V.N. Lyashchenko, A.O. Mytsykov, L.V. Onischenko // Problems of atomic science and technology. — 2019. — № 2. — С. 145-150. — Бібліогр.: 27 назв. — англ.
series Вопросы атомной науки и техники
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fulltext ISSN 1562-6016. PASТ. 2019. №2(120), p. 145-150. RARE-EARTH PERMANENT MAGNET IN MAGNETIC SYSTEM OF ELECTRON ACCELERATOR WITH THE ENERGY OF 10 MеV V.A. Bovda, A.M. Bovda, I.S. Guk, S.S. Kandybey, S.G. Kononenko, V.N. Lyashchenko, A.O. Mytsykov, L.V. Onischenko National Science Center “Kharkov Institute of Physics and Technology”, Kharkov, Ukraine E-mail: bovda@kipt.kharkov.ua The radiation resistance of Sm-Co and Nd-Fe-B magnets under 10 MeV electron beam was studied. The simula- tion and design of a magnetic system for electron beam analysis of a technological accelerator for energy up to 10 MeV was carried out. The key component of magnetic system was Sm2Co17 magnets with the size of 30х24х12 mm. The maximum magnetic field in the magnetic system was 0.3 T. PACS: 29.30.Kv INTRODUCTION There is a considerable interest in the magnetic sys- tems on the base of rare-earth permanent magnets for use in special accelerators such as medical and techno- logical accelerators, microtrons, liner colliders and etc [1–5]. The creation of each such device is associated with the need to take into account the parameters of accelerators and the features of their operation. The key component of the accelerating unit is permanent mag- nets. The magnetic performance, time and thermal sta- bility of the magnetic materials under irradiation play crucial role for the steady operational parameters. Linear accelerator LU-10 [6] in the NSC KIPT has been used for many years for technological radiation treatment of materials. Now, significant upgrade of all the accelerator systems is performed. The main beam parameter of this accelerator [7] after system upgrading – maximum energy must be near 9.44 MeV. The up- grading beam parameters were used in selecting the basic requirements for a magnetic system aimed at measuring the energy of the accelerator beam [8, 9]. According to the simulation and experimental meas- urements, the design of the magnet should provide a field of about 0.3 T in a gap of 2.5 cm. The choice of magnetic material for use in a magnet- ic system has been made. The paper also presents the results of the development of the design and experi- mental details of the magnetic characteristics of magnet- ic system. 1. THE CHOICE OF MAGNET MATERIAL One of the practical aspects of permanent magnets using in the technological accelerators is the high radia- tion background. Thus, magnetic materials should pre- serve magnetic performance under high radiation doses induced by electron beam and bremsstrahlung. Despite an extensive literature on radiation stability of Sm-Co and Nd-Fe-B magnets under electron irradiation with energy from 8 GeV to 10 MeV and gamma-radiation [10–23], the selection of appropriate magnetic material can be described relatively unambiguously. According- ly, experimental study of magnetic losses of Sm-Co and Nd-Fe-B magnets under direct electron beam irradiation with the energy of 10 MeV and bremsstrahlung were carried out [24, 25]. Permanent magnets were produced by powder met- allurgy [26]. Magnetic samples were magnetized to the technical saturation in the magnetic field of 3.5 T. Typi- cal size of rectangular magnets was 30×24×12 mm. Nd-Fe-B magnets were covered with Ni coating. Samples were irradiated by electron beam with en- ergy of 10 MeV on the linear technological accelerator KUT-1 [27]. The axis of accelerator was located verti- cally. The electron beam yield was from top to down. Electron beam passed to the air through the titanium foil. In the experiment, the south pole of Nd-Fe-B mag- nets (30×24 mm side) underwent electron irradiation. The deviation of electron beam density was about 10% above the sample’s surface. During the electron irradia- tion, magnets were cooled by the water. The tempera- ture of the coolant water was not less than 40 °С. Four (4) Nd-Fe-B and four (4) Sm-Co magnets were used in experiments. The following designation was used for both types of magnets. Samples 1 and 2 were irradiated continuously for 20 hours. Electron beam went directly to the surface of sample 1. The absorbed dose for the sample 1 was 16 Grad (the total electron flux was of about 1.4∙10 17 electrons/сm 2 ). Sample 2 was irradiated simultaneously with the sample 1, but sample 2 was set far from the electron beam at the distance of 40 mm. Sample 3 was irradiated for 20 hours with 24 intervals. The total absorbed dose for the sample 3 was 160 Grad. Sample 4 was not irradiated and it was used as the reference sample for the measurements. It was revealed that Nd-Fe-B magnets had a small amount of 147 Nd unstable isotope. It is the result of 148 Nd(γ, n) 147 Nd reaction with the energy threshold of 7.3 MeV and half lifetime of 10.98 days. The radiation spectrum of Sm-Co magnets was characterized by the 153 Sm isotope produced by 154 Sm(γ, n) 153 Sm reaction under gamma-radiation of electron bremsstrahlung. The isotope half lifetime is 46.284 hours. Thus, the activity of the magnets after the irradiation was within normal range. The latter allows normal operation of the devices with Nd-Fe-B and Sm-Co magnets in accelerators with the energy up to 10 MeV. 2. MAGNETIC MEASUREMENTS The measurements of the normal z-component of magnetic flux were performed using Hall probe line (HPL) [24]. Hall probes were mounted into the cupper matrix for temperature compensation. The distance be- tween Hall probes on the HPL was about 6 mm. The accuracy of measurements was about 0.03%. The sample was passed transversely to the HPL. The distance between magnets and HPL was 3.05 mm. Magnets passed over the HPL with the step from 3 to 5 mm. The precision of magnet’s position was about 1 μm. The initial position of the sample within HLP was fixed by stoppers. HLP measurements were performed on the both sides of the magnet (north pole and south pole). 3D quadratic interpolation can be used to estimate approximation of magnetic field gradients along the plane of a magnet. The approximation was done using the measured HPL data. The interpolation area was set by the distance between outermost probes of HPL and x-y scanning area. The scanning area was precisely de- termined by the sample coordinate system. Fig. 1 shows the interpolation results for the HPL collected data for non-treated Nd-Fe-B sample 1. Fig. 1. Interpolation of the experimental data for the Nd-Fe-B magnet (sample 1) before irradiation In order to estimate the changes in magnetic flux, the integral of the 3D interpolation normal component of magnetic flux was used. Calculated S-parameter measured in arbitrary units was chosen as integrated z-component of magnetic flux. The S-parameter is cal- culated within the x-y plane of the magnet. The relative error for S-parameter is about 0.5% within HPL bound- aries. The S-parameters of Nd-Fe-B magnets (north pole) before electron irradiation are shown in the Tabl. 1. It was revealed that S-parameter for both poles (south and north) coincided within the experiment accuracy. Table 1 S-parameter (integrated z-component of magnetic flux) of Nd-Fe-B magnets before and after electron irradiation Sample S, a.u. Initial e-irradiated north pole* north pole south pole 1 175.763 162.356 160.2 2 179.556 178.526 – 3 176.357 126.556 – 4 175.452 – – *North and south pole coincides within relative error. The interpolations of magnetic field distribution of the sample 1 (north pole and south pole) after electron irradiation are depicted in Figs. 2 and 3, accordingly. One can see that S value was decreased to 162.356 and 160.2. Fig. 2. Interpolation of the experimental data for the north pole of Nd-Fe-B magnet (sample 1) after irradia- tion. Absorbed dose of 16 Grad Fig. 3. Interpolation of the experimental data for the south pole of Nd-Fe-B magnet (sample 1) after irradia- tion. Absorbed dose of 16 Grad As can be seen in Figs. 2 and 3, magnetic field dis- tribution and S-parameters coincided for both poles of the magnet (sample 1) within the accuracy of measure- ments. Fig. 4. Interpolation of the experimental data for the north pole of Nd-Fe-B magnet (sample 2) after brems- strahlung irradiation. Absorbed dose of 16 Grad The magnetic field distribution for the sample 2 after bremsstrahlung irradiation was the same as before irra- diation (Fig. 4) and the S-parameter of 178.526 was practically the same. The substantial changes in the magnetic field distri- bution after irradiation were observed for sample 3 (Fig. 5). The S-parameter for the sample 3 was de- creased to 126.556. It should be noticed that reduction of S-parameter was not proportional to the absorbed dose. Fig. 5. Interpolation of the experimental data for the north pole of Nd-Fe-B magnet (sample 3) after irradia- tion. Absorbed dose of 160 Grad For the reference sample 4, the magnetic field distri- bution measurements after the end of the measurement cycle on the irradiated samples showed a coincidence with the distributions obtained before irradiation. The similar magnetic measurements were done for Sm-Co magnets. The S-parameters are as following the south pole for the sample 1 is 151.94, for the sample 2 is 149.007, for the sample 3 is 152.326, for the sample 4 is 152.519 (Tabl. 2). The S-parameters of north pole were the same as for the south pole within experiment accu- racy. The interpolation of the magnetic field distribution of Sm-Co magnet (sample 1) before irradiation is shown in Figs. 6 and 7. Table 2 S-parameter (integrated z-component of magnetic flux) of Sm-Co magnets before and after electron irradiation Sample S, a.u. Initial e-irradiated south pole* north pole south pole 1 151.94 – – 2 149.007 148.397 149.727 3 152.326 149.714 150.065 4 152.519 152.496 155.135 *North and south pole coincides within relative error. B, T x y Fig. 6. Interpolation of the experimental data for the south pole of Sm-Co magnet (sample 1) before irradiation y x B, T Fig. 7. Interpolation of the experimental data for the north pole of Sm-Co magnet (sample 1) before irradiation The distribution of the magnetic field of Sm-Co magnet (sample 1) left unchanged after irradiation (Fig. 8). B, T x y Fig. 8. Interpolation of the experimental data for the north pole of Sm-Co magnet (sample 1) after irradia- tion. Absorbed dose of 16 Grad It was revealed that the absorbed dose of 160 Grad for the sample 3 did not change the initial magnetic field distribution around the magnet. The S-parameter of sample 2 was 148.397 and 149.727, for the sample 3 was 149.714 and 150.065 for the north and south poles respectively. The magnetic field distributions of refer- ence samples were not changed during experiments. Despite high absorption doses, Sm-Co magnets (sample 2 and sample 3) preserved their magnetic performance. The S-parameter of untreated Sm-Co magnet (sample 4) was 152.496 and 155.135, correspondingly. Thus, it was shown the advantage of using Sm-Co magnets, because their magnetic properties did not change under direct irradiation with an electron beam and bremsstrahlung. In addition, Sm2Co17 magnets have better magnetic characteristics under critical conditions as the device should remain stable. Such conditions can often arise when magnets are used on technological electron accel- erators. In the case of operation under high temperatures and aggressive conditions, Sm2Co17 alloy have certain advantages over devices made of Nd-Fe-B alloy. The Curie temperature of the Sm2Co17 alloy is Tc = 825 0 C. The maximum operating temperature of the Sm-Co magnets reaches Tw = 350 0 C. The Curie temperature of the Nd-Fe-B magnet is Tc = 312 0 C. Thus, under real experimental conditions the operating temperatures for this alloy should not exceed Tw = 180 0 C. The temperature stability of Nd-Fe-B magnets is smaller than that of Sm-Co magnets. The temperature coefficient of magnetic induction (Br) of Nd-Fe-B mag- nets varies from 0.07 to 0.13 %/ 0 C, in contrast to 0.035 %/ 0 C in Sm-Co magnets. In addition, Sm-Co magnets are less prone to corrosion than neodymium magnets, and usually do not require coating. Hence, Sm-Co magnets were chosen for the development of a magnet system for electron accelerator. 3. MAGNETIC SYSTEM DESIGN To assess the parameters of magnetic system, the simulation of beam travel at the output of the accelera- tor was carried out. The parameters of the beam and magnetic field inside magnetic system were fixed. The typical size of Sm-Co magnets for the design of magnet- ic systems was 30×24×12 mm. The distance between Sm-Co magnets was 25 mm. The typical magnetic field in the mid-plane of the magnetic system was about 0.3 T. This peak magnetic field of 0.3 T was used for the simulation of beam travel. Hence, the simulation allowed designing the construction of magnetic system. Fig. 9. Magnetic system for electron accelerator Fig. 9 shows the magnetic system which was de- signed and constructed according simulation experi- ments. Outside dimensions of the magnetic circuit were 90x73x24 mm. The magnetic circuit was made of soft magnetic steel. Sm-Co magnets were fixed to the bar by aluminum clamps. The tolerance and machining of parts were of 5 m. The upper bar was designed portable to facilitate the dismantling of the magnetic system and the flange of accelerator during the measuring mode or ad- justment accelerator energy procedure. The design of the magnetic system provides the dispersion of magnet- ic field in the both horizontal and vertical directions. The distribution of magnetic field in the magnetic system was carried out by abovementioned HPL meth- od. Fig. 10 shows the experimental plot of HPL data. The mid-plane scans in the gap of magnetic system on the base of Sm-Co magnets are shown in Fig. 11. It was found that peak magnetic field in the gap of magnetic system was 0.331103 T. The effective length along the central line of beam track was – 33.533 mm. The rota- tion angle of electron beam with the energy of 10 MeV was 0.31 rad. The estimation of the rotation angle was done according to the simulation of electron beam mo- tion. Fig. 10. The distribution of magnetic field of magnetic system on the base of Sm-Co magnets. Experimental HPL plot The deviation of magnetic field in the gap of mag- netic system was investigated under various regimes as opening and closing circuit, and the reconfiguration of the upper bar. Fig. 12 shows the measurements of seven Hall probes in the gap of magnetic system during 10 cycles of opening and closing circuit for 1000 s. Fig. 11. Magnetic field distribution in the mid-plane of gap of magnetic system on the base of Sm-Co magnets (interpolation of HPL data) Fig. 12. The distribution of magnetic field in the mag- netic system after one cycle of opening/closing circuit Fig. 13. The change of magnetic field (Hall probe data) after each cycle of closing and opening circuit The relative change of the magnetic field at the measurement points is shown in Fig. 13. Hall probes located at the centre of the magnetic system (green, red and pink points) showed magnetic field variation about 0.5% after closing circuit. CONCLUSIONS In summary, it was revealed that Sm-Co magnets had advantage in preserving magnetic performance un- der high electron irradiation and bremsstrahlung. The optimal design of magnetic system for particular elec- tron accelerator with the energy of 10 MeV was devel- oped. The measured parameters of the magnetic system agreed with the simulation experiment. REFERENCES 1. V.I. Shvedunov et al. A 70 MeV Race-Track Mi- crotron // Nucl. Instr. Meth. 2005, v. 550, N 1-2, p. 39- 53. 2. David J. McLaughlin et al. 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Приведены результаты экспериментального исследования харак- теристик магнита. Максимальное поле в магните равно 0,3 Тл. ВИКОРИСТАННЯ РІДКІСНОЗЕМЕЛЬНИХ ПОСТІЙНИХ МАГНІТІВ У МАГНІТНІЙ СИСТЕМІ ЕЛЕКТРОННОГО ПРИСКОРЮВАЧА НА ЕНЕРГІЮ 10 МеВ В.О. Бовда, О.М. Бовда, І.С. Гук, С.С. Кандибей, С.Г. Кононенко, В.М. Лященко, А.О. Мициков, Л.В. Оніщенко Експериментально досліджена радіаційна стійкість магнітних матеріалів зi Sm-Co- і Nd-Fe-B-сплавів під дією 10 МэВ електронного пучка. На основі зразків зi Sm2Co17-сплаву розмірами 30х24х12 мм проведені моделювання і конструювання магніту для аналізу пучка електронів технологічного прискорювача на енер- гію 10 МеВ. Приведено результати експериментального дослідження характеристик магніту. Максимальне поле в магніті дорівнює 0,3 Тл.