Facile and scalable synthesis of Ti₅Si₃ nanoparticles via solid-state route in an autoclave
A novel method of the synthesis of titanium silicide nanoparticles via solid-state route in an autoclave at 700 °C is reported. The reaction of titanium silicide could be described briefly as: 5TiO₂ + 3Si + 20Li = Ti₅Si₃ + 10Li₂O. XRD pattern indicated that the product was hexagonal Ti₅Si₃. The Ti₅S...
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| Date: | 2017 |
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| Main Authors: | , , , , , , |
| Format: | Article |
| Language: | English |
| Published: |
Інститут надтвердих матеріалів ім. В.М. Бакуля НАН України
2017
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| Series: | Сверхтвердые материалы |
| Subjects: | |
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| Journal Title: | Digital Library of Periodicals of National Academy of Sciences of Ukraine |
| Cite this: | Facile and scalable synthesis of Ti₅Si₃ nanoparticles via solid-state route in an autoclave / W. Mao, K. Bao, F. Cao, L. Ye, H. Xie, B. Li, W. Wang // Сверхтвердые материалы. — 2017. — № 2. — С. 56-61. — Бібліогр.: 21 назв. — англ. |
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Digital Library of Periodicals of National Academy of Sciences of Ukraine| Summary: | A novel method of the synthesis of titanium silicide nanoparticles via solid-state route in an autoclave at 700 °C is reported. The reaction of titanium silicide could be described briefly as: 5TiO₂ + 3Si + 20Li = Ti₅Si₃ + 10Li₂O. XRD pattern indicated that the product was hexagonal Ti₅Si₃. The Ti₅Si₃ particle size (about 20–40 nm) is confirmed by the TEM images. Furthermore, the thermal stability and oxidation resistance of the titanium silicide nanoparticles were also investigated. |
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